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장비 상세조회

X-선 회절분석기
X-Ray Diffractometer

영문약어 XRD
장비명(한글) X-선 회절분석기 
기기코드 SC222
연구장비표준분류
기기상태 양호 
SC222.jpg

부서 및 장비담당자

부서 및 장비담당자
지역 서울센터 
주소 (02855)
서울특별시 성북구 인촌로 22길 6-7 고려대학교 자연캠퍼스 내 한국기초과학지원연구원 
보유센터 및 부서 서울센터 환경대응연구팀 
장비담당자 정슬기, 윤혜온, 김도영
전화 02-6943-4194, 02-6943-4192, 02-6943-4127 
팩스  
메일 sjeong85@kbsi.re.kr  

Spec 및 활용분야

원리 및 특징
    · X-선이 어떤각도 θ로 결정표면에 부딪칠 때, 표면의 원자층에 의해 X-선이 산란되며 산란되지 않은 부분의 X-선은 원자의 다음층으로 침투하는데, 그 일부 X-선은 다시 산란된다. 일정한 간격으로 놓여 있는 결정 중심에서 생기는 이런 산란의 종합적인 효과가 X-선 회절이며 입사하는 X-선이 Bragg 법칙을 만족할 때 얻어지는 X-선 회절상으로 무기물의 조성분석 및 결정 구조를 분석한다.
구성 및 성능
    ○ X-ray generator : 3㎾ (Cu anode)
    ○ High temperature attachment (실온 ∼ 1600℃)
    ○ Low temperature attachment (80K ∼ 620K)
    ○ Thin film detector 장착으로 박막의 측정에 용이
    ○ Twin vertical goniometer system
활용분야
    ○ 박막, bulk 및 분말 무기물 시료의 결정상 측정
    ○ 분말회절상을 이용한 결정구조: 토양, 암석 내 광물 및 각 광물의 결정구조 분석
    ○ 합성 화합물의 구조분석(소재공학): GaN, Ni-Fe, Mn-Cu-Co 산화물 등의 합성 화합물의 구조 분석
    ○ 합성물의 결정성분석: 시료 크기 범위(~20㎛) 이하의 결정 또는 비결정질 물질인지의 여부 분석
    ○ 유물의 과학적 연구 지원: SiO2 및 주요 점토광물의 구조 분석을 통한 기와 및 도자기 등 유물의 제작 온도 등의 연구

장비 공지사항


연관논문

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Synthesis and magnetic characterization of a cubane-type Mn4 cluster, housed in a sterically hindered carboxylate ligand pocket
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Selective catalytic oxidation of H2S over V2O5-supported Fe-pillared montmorillonite clay
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CATALYSIS TODAY, 2011
PPV Nanotubes, Nanorods and Nanofilms and Carbonized Objects Derived Therefrom
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ACS Symposium Series, 874, 2004
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Ferromagnetic Mn-doped GaN nanowires
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Appl. Phys. Lett., 2005
Influence of In incorporation on the electronic structure of ZnO nanowires
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APPLIED PHYSICS LETTERS, 2005
Comparative Structure and Optical Properties of Ga-, In-, and Sn-Doped ZnO Nanowires Synthesized via Thermal Evaporation
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Single- and Double-Shelled Coaxial Nanocables of GaP with Silicon Oxide and Carbon
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Short-Period Superlattice Structure of Sn-Doped In2O3(ZnO)4 and In2O3(ZnO)5 Nanowires
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J. Phys. Chem. B, 2005
Magnetic Properties of Monodisperse NiHx Nanoparticles and Comparison to Those of Monodisperse Ni Nanoparticles
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J. Phys. Chem. B, 2005
Ferrimagnetism in Manganese Sesquioxide Mn2O3 Nanoparticles
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Journal of the Korean Physical Society, 2005
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Journal of the Korean Physical Society, 2005
Effects of oxygen-plasma treatment in La0.7Ca0.3MnO3-£ thin films
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A series of long-chain lamellar hydrated copper(II) alkylsulfonates with different chain molecular assemblies
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APPLIED PHYSICS LETTERS, 2005
Electronic Structure and Field Emission of Multiwalled Carbon Nanotubes Depending on Growth Temperature
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J. Phys. Chem. B, 2005
Synthesis and magnetic properties of Zn1-xMnxO films prepared by the sol-gel method
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Solid State Communications, 2004
Vertically Aligned Sulfur-Doped ZnO Nanowires Synthesized via Chemical Vapor Deposition
Seung Yong Bae, Hee Won Seo, and Jeunghee Park
Journal of Physical Chemistry B, 2004
Heterostructures of ZnO Nanorods with Various One-Dimensional Nanostructures
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Journal of Physical Chemistry B, 2004
Synthesis of blue-light-emitting ZnGa2O4 nanowires using chemical vapor deposition
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Chemical Communication, 2004
Layered Copper Hydroxide n-Alkylsulfonate Salts: Synthesis, Characterization, and Magnetic Behaviors in Relation to the Basal Spacing
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Applied Physics Letters, 2004
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Effects of sputtering pressure on the characteristics of lithium ion conductive lithium phosphorous oxynitride thin film
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Large-scale synthesis of gallium nitride nanosaws using a chemical vapor deposition method
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Chemical Physics Letters, 2003
Triangular gallium nitride nanorods
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Applied Physics Letters, 2003
Boron nitride nanotubes synthesized in the temperature range 1000–1200 °C
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Chemical Physics Letters, 2003
Porous GaN nanowires synthesized using thermal chemical vapor deposition
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Chemical Physics Letters, 2003
Nitrogen-doped gallium phosphide nanobelts
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Applied Physics Letters, 2003
Direct Synthesis of Gallium Nitride Nanowires Coated with Boron Carbonitride Layers
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Chemical Physics Letters, 2003
Controlled Structure of Gallium Oxide Nanowires
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Chemical Physics Letters, 2003
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CHEMICAL PHYSICS LETTERS, 2003
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CHEMICAL PHYSICS LETTERS, 2003
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Ferromagnetism of MnO and Mn3O4 nanowires
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Applied Physics Letters, 2005
Strained gallium nitride nanowires
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Chemical Communications, 2002
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Chanrge modulation spectra in phosphorus-doped a-Si:H
Lyou jong hun
J.Non-crysr. Solids, 2000
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Tin Solid Films, 2000
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MRS Symposium proceedings,San Francisco(Aprill,1999), 1999
Infrared electroabsorption spectra in amorphous silicon solar cell
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the role of thin amorphous silicon layer on the fabrication of micro-pored silicon
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Visible photoluminescence from an anodized polycrrystalline silicon thin film/silicon structure.
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J.kor.Phy.Soc., 1997
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Low Temperature Growth and Photoluminescence of Well-aligned Zinc Oxide Nanowires
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