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600MHz 온라인액체크로마토그라피 핵자기공명질량분석기 시스템
600 MHz Online LC-NMR-MS System

분석장비 상세내역
영문약어 LC-NMR-MS
장비명(한글) 600MHz 온라인액체크로마토그라피 핵자기공명질량분석기 시스템 
기기코드 KJ206
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광주광역시 북구 용봉로 77 전남대학교 내 한국기초과학지원연구원 
보유센터 및 부서 광주센터 분석연구부 
장비담당자 이영주  박기덕  김지윤  
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Spec 및 활용분야

Spec 및 활용분야
원리 및 특징
    · Rapid dereplication and structural identification of complex mixtures can be facilitated by direct hyphenation of three analytical methods(LC-NMR-MS) and high sensitivity of the state-of-the-art cryogenic probe
구성 및 성능
    ○ Superconductor Magnet (14.1 T)
    ○HPLC
    ○ Mass Spectrometer
    ESI/APcI Triple Quadruple Mass (MS/MS)
    ○ Carbon enhanced cryogenic Probe
    Sensitivity of 1H - 4700:1
    Sensitivity of 13C - 500:1
활용분야
    ○ Natural Products Biomedical and Pharmaceuticals
    - Drug metabolism and related research
    ○ Functional foods
    ○ 혼합물의 온라인 분석, 화학 구조분석전화 상담

    기기문의 : 062-530-0513, 0517
    행정문의 : 062-530-0516

장비 공지사항


연관논문

Electrocatalytic Production of C3-C4 Compounds by Conversion ofCO2on aChloride-Induced Bi-Phasic Cu2O-Cu Catalyst
Seunghwa Lee, Dahee Kim, and Jaeyoung Lee
ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2015
Sustainable production of formic acid by electrolytic reduction of gaseous carbon dioxide
Seunghwa Lee, HyungKuk Ju, Revocatus Machund, Sunghyun Uhm, Jae Kwang Lee, Hye Jin Lee and Jaeyoung Lee
Journal of Materials Chemistry A, 2015
A Phenyl Lipid Alkaloid and Flavone C-Diglucosides from Spergularia marina
Jeong-Yong Cho, Min-Su Kim, Yu Geon Lee, Hang Yeon Jeong, Hyoung Jae Lee, Kyung-Sik Ham, and Jae-Hak Moon
Food science biotechnology, 2016
Isolation and Antioxidative Activity of Amino Acid Derivatives Produced by Leuconostoc mesenteroides
Yu Geon Lee, Jeong-Yong Cho, and Jae-Hak Moon
Food science biotechnology, 2016
Isolation and Identification of Two Flavonoids from Pear (Pyrus pyrifolia Nakai cv. Chuhwangbae) Fruit Peel
이상원, 이유건, 조정용, 김영출, 이상현, 김월수, ·문제학
한국식품과학회지, 2015
Establishment of a simple method for purification of high purity chlorogenic acid from immature fruit of pear (Pyrus pyrifolia Nakai)
Sang Won Lee, Yu Geon Lee, Jeong-Yong Cho, Young Choll Kim, Sang-Hyun Lee, Wol-Soo Kim, Jae-Hak Moon
The Korean Society for Applied Biological Chemistry, 2015
Cytotoxic Components in an Extract from the Leaves and Stems of Stauntonia hexaphylla
Jing Zhao, 임순호, 엄정인, 박시환, 오은상, 정다운, Darren R. Williams, 이익수
Natural Product Sciences, 2014
Coumaroyl Quinic Acid Derivatives and Flavonoids from Immature Pear (Pyrus pyrifolia Nakai) Fruit
Yu Geon Lee, Jeong-Yong Cho, Chan-Mi Kim, Sang-Hyun Lee, Wol-Soo Kim, Tae-Il Jeon, Keun-Hyung Park,
FOOD SCIENCE AND BIOTECHNOLOGY, 2013
Isolation and Identification of 3 Low-molecular Compounds from Pear (Pyrus pyrifolia Nakai cv. Chuhwangbae) Fruit Peel
Yu Geon Lee, Jeong-Yong Cho, Chan-Mi Kim, Hang-Yeon Jeong, DongI Lee, Soo Ro Kim, Sang-Hyen Lee, Wol
Korean Society of Food Science and Technology, 2013
Isolation and Identification of a Sterol and Three Glucosides from the Peel of Pear (Pyrus pyrifolia Nakai cv. Chuhwangbae)
Yu Geon Lee, Jeong-Yong Cho, Hyun Joo Lee, Yong Hyun Lee, Sang-Hyun Lee, Tae-Ho Han, Wol-Soo Kim, Ke
한국식품과학회지, 2013
Isolation and Identification of Antioxidative Compounds and Their Activities from Suaeda japonica
Jeong-Yong Cho, Xing Yang, Kyung-Hee Park, Hye Jin Park, Sun-Young Park, Jae-Hak Moon, and Kyung-Sik
FOOD SCIENCE AND BIOTECHNOLOGY, 2013
Three New Lignan Glycosides with IL-6 Inhibitory Activity from Akebia quinata
Hong-Guang Jin, A Ryun Kim, Hae Ju Ko, Sang Kook Lee, and Eun-Rhan Woo
Chemical and Pharmaceutical Bulletin, 2014
Phenolic compounds with IL-6 inhibitory activity from Aster yomena
A Ryun Kim, Qinglong Jin, Hong-Guang Jin, Hae Ju Ko, Eun-Rhan Woo
ARCHIVES OF PHARMACAL RESEARCH, 2014
Caffeoyl Triterpenes from Pear (Pyrus pyrifolia Nakai) Fruit Peels and Their Antioxidative Activities against Oxidation of Rat Blood Plasma
1. Jeong-Yong Cho, Chan Mi Kim, Hyoung Jae Lee, Sang-Hyun Lee, Jeong-An Cho, Wol-Soo Kim, Keun-Hyung
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2013
Coumaroyl Quinic Acid Derivatives and Flavonoids from Immature Pear (Pyrus pyrifolia Nakai) Fruit
Yu Geon Lee, Jeong-Yong Cho, Chan-Mi Kim, Sang-Hyun Lee, Wol-Soo Kim, Tae-Il Jeon, Keun-Hyung Park,
FOOD SCIENCE AND BIOTECHNOLOGY, 2013
Large-scale Isolation of Highly Pure Malaxinic Acid from Immature Pear (Pyrus pyrifolia Nakai) Fruit
Yu Geon Lee, Jeong-Yong Cho, Jun Park, Sang-Hyun Lee, Wol-Soo Kim, Keun-Hyung Park, and Jae-Hak Moon
FOOD SCIENCE AND BIOTECHNOLOGY, 2013
추황배(Pyrus pyrifolia Nakai cv. Chuhwangbae) 과피로부터 1종의 Sterol과 3종의 배당체 화합물의 단리·동정
이유건, 조정용, 이현주, 이용현, 이상현, 한태호, 김월수, ·박근형, 문제학
korean jounal of food science and technology, 2013
추황배(Pyrus pyrifolia Nakai cv. Chuhwangbae) 과피로부터 3종의 저분자 화합물의 단리·동정
이유건, 조정용, 김찬미, 정항연, 이동이, 김수로, 이상현, 김월수, 박근형, 문제학
korean jounal of food science and technology, 2013
Quantitative analyses of individual g-Oryzanol (Steryl Ferulates) in conventional and organic brown rice (Oryza sativa L.)
Jeong-Yong Cho, Hyoung Jae Lee, Gee An Kim, Gwi Deok Kim, You Seok Lee, Soo Cheol Shin, Keun-Hyung P
JOURNAL OF CEREAL SCIENCE, 2013
Diterpene glycosides from Korean fermented red pepper paste (gochujang) and their origin
Heung-Chule Shin, Jeong-Yong Cho, Ki Hoon Lee, Young-Kyu Ma, Jong Hoon Jeong, Hyoung Jae Lee,
FOOD CHEMISTRY, 2013
Caffeoyl Triterpenes from Pear (Pyrus pyrifolia Nakai) Fruit Peels and Their Antioxidative Activities against Oxidation of Rat Blood Plasma
Jeong-Yong Cho, Chan Mi Kim, Hyoung Jae Lee, Sang-Hyun Lee, Jeong-An Cho, Wol-Soo Kim, Keun-Hyung Pa
JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2013
An Ether and Three Ester Derivatives of Phenylpropanoid from Pear (Pyrus pyrifolia Nakai cv. Chuhwangbae) Fruit and Their Radical-Scavenging Activity
Jeong-Yong Cho, Yu Geon Lee, Sang-Hyun Lee, Wol-Soo Kim, Keun-Hyung Park, and Jae-Hak Moon
Food Science Biotechnol, 2013
Isolation and Identification of Phenolic Compounds from an Asian Pear (Pyrus pyrifolia Nakai) Fruit Peel
Ki Hoon Lee, Jeong-Yong Cho, Hyoung Jae Lee, Keun Young Park, Young-Kyu Ma, Sang-Hyun Lee,Jeong An C
FOOD SCIENCE AND BIOTECHNOLOGY, 2011
Isolation and Structural Determination of Antioxidants from EtOAc Acidic Fraction of Pear Extract
이기훈
전남대학교, 2011
Curcuminoids from Curcuma longa and their inhibitory activities on Influenza A neuraminidases
Dao TT, Nguyen PH, Won HK, Kim EH, Park J, Won BY, Oh WK
FOOD CHEMISTRY, 2011
Synthesis of 12-oxobenzo[c]phenanthridinones and 4-substituted 3-arylisoquinolones via Vilsmeier-Haack reaction
Daulat Bikram Khadka, Su Hui Yang, Suk Hee Cho, Chao Zhao, Won-Jea Cho *
TETRAHEDRON, 2012
Structure-Guided Identification of Novel Phenolic and Phenolic Amide Allosides from the Rhizomes of Cimicifuga heracleifolia
Soon-Ho Yim, Hyun Jung Kim, Nari Jeong, Ki Deok Park, Young Ju Lee, Sung Dong Cho, Ik-Soo Lee
BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 2012
Cytotoxic Caffeic Acid Derivatives from the Rhizomes of Cimicifuga heracleifolia
Soon-Ho Yim, Hyun Jung Kim, Si-Hwan Park, Jinmi Kim, Darren R. Williams, Da-Woon Jung, Ik-Soo Lee
ARCHIVES OF PHARMACAL RESEARCH, 2012
Copper-Catalyzed One-Pot Three-Component Synthesis of Benzimidazoles by Condensation and C-N Bond Formation
김용, Manian Rajesh Kumar, 박남진, 허유미, 이선우
J. Org. Chem., 2011
Characterization of Nanoporous Cavity of Quardruply Bridged Calix[6]arenes by Means of Hyperpolarized Xe-129 NMR
이영주,박기덕, 여형민, 류병주, 남계춘, 하토리 미테유끼
Journal of Nanoscience and Nanotechnology, 2010
Metabolism and antioxidant effect of malaxinic acid and its corresponding aglycone in rat blood plasma
Hyun JooLee,Hang YeonJeong,Mi RimJin,Hyoung JaeLee,Jeong YongCho,Jae HakMoon
Free Radical Biology and Medicine, 2017
Palladium-Catalyzed Decarboxylative Coupling of Alkynyl Carboxylic Acids with Aryl Tosylates
Lee, J.-H. Raja, G. C. E. Yu, S. Lee, J. Song, K. H. Lee, S.
ACS Omega, 2017
Expression, Purification and Characterization of the BLM binding region of human Fanconi Anemia Group J protein
염규호, 박진주
Journal of the Korean Magnetic Resonance Society, 2016
Room temperature cyclization of arylpropiolic acid anhydride: Synthesis of naphtho[2,3-c]furan-1,3-dione derivatives
Jaerim Park, Ji Dang Kim, Gabriel Charles Edwin Raja, Hyun Chul Choi, Sunwoo Lee
SYNTHETIC COMMUNICATIONS, 2017
Discovery of Isoquinolinoquinazolinones as a Novel Class of Potent PPARγ Antagonists with Anti-adipogenic Effects
Yifeng Jin*, Younho Han*, Daulat Bikram Khadka, Chao Zhao, Kwang Youl Lee & Won-Jea Cho
Scientific Reports, 2016
Design and synthesis of novel androgen receptor antagonists via molecular modeling
Chao Zhao, You Hee Choi, Daulat Bikram Khadka, Yifeng Jin, Kwang-Youl Lee, Won-Jea Cho
BIOORGANIC & MEDICINAL CHEMISTRY, 2016
Change in Flavonoid Composition and Antioxidative Activity during Fermentation of Onion (Allium cepa L.) by Leuconostoc mesenteroides with Different Salt Concentrations
Yu GeonLee,Jeong YongCho,Young MinKim,Jae HakMoon
Journal of food science, 2016
Isolation and antioxidative activity of amino acid derivatives produced by Leuconostoc mesenteroides
Yu GeonLee,Jeong YongCho,Jae HakMoon
Food Science and Biotechnology, 2016
A phenyl lipid alkaloid and flavone C-diglucosides from Spergularia marina
Jeong YongCho,Jeong YongCho,Min SuKim,Yu GeonLee,Hang YeonJeong,Hyoung JaeLee,Kyung SikHam,Jae HakMoon
FOOD SCIENCE AND BIOTECHNOLOGY, 2016
Nickelbriphos-catalyzed transamidation of unactivated tertiary amides
DahyeonYang, TaeilShin, HyunwooKim, SunwooLee,
ORGANIC & BIOMOLECULAR CHEMISTRY, 2020
Discovery of orally active indirubin-3′-oxime derivatives as potent type 1 FLT3 inhibitors for acute myeloid leukemia.
Jeong, P., Moon, Y., Lee, J., Lee, S., Park, J., Lee, J., Kim, J., Lee, H., Kim, N., Choi, J., Heo, J., Shin, J., Park, H., Kim, Y., Han, S. and Kim, Y.
EUROPEAN JOURNAL OF MEDICINAL CHEMISTRY, 2020
Dual Rh(II)Pd(0) Relay Catalysis Involving Sigmatropic Rearrangement Using N-Sulfonyl Triazoles and 2-Hydroxymethylallyl Carbonates
Liang-Zhu Huang, Zi Xuan, Jong-Un Park, and Ju Hyun Kim
ORGANIC LETTERS, 2022
Biotransformation of the phenolic constituents from licorice and cytotoxicity evaluation of their metabolites
YinaXiao, FuboHan, Ik SooLee,
INTERNATIONAL JOURNAL OF MOLECULAR SCIENCES, 2021
Formation of a tris(catecholato) iron(iii) complex with a nature-inspired cyclic peptoid ligand
JinyoungOh, DahyunKang, SugyeongHong, Sun H.Kim, Jun HoChoi, JiwonSeo,
DALTON TRANSACTIONS, 2021

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